• Title/Summary/Keyword: Mineral powder

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Preparation of Low-Oxygen Ingot by Repetitive Melting and Mo Metal Powder by Hydrogen Reduction from $MoO_3$ Powder (삼산화 몰리브덴 분말로부터 수소 환원에 의한 금속 분말 및 반복 용해에 의한 저산소 잉곳 제조)

  • Lee, Back-Kyu;Oh, Jung-Min;Kim, Hyung-Seok;Lim, Jae-Won
    • Particle and aerosol research
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    • v.9 no.1
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    • pp.31-36
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    • 2013
  • In this study, Mo metal powder was prepared by hydrogen reduction of Mo trioxides with different purity of 2N and 3N grades. We have obtained Mo metal powder with oxygen content of 1450 ppm by hydrogen reduction and subsequent heat treatment for degassing. Using the Mo metal powder, a low-oxygen Mo ingot was prepared by repetitive vacuum arc melting. The oxygen content of the obtained Mo ingot was less than 70 ppm after vacuum arc melting for 30 min. The purity of the Mo metal powder and the ingot was evaluated using glow discharge mass spectrometry. The purity of the respective Mo ingots was increased to 3N and 4N grades from the Mo powder of 2N and 3N grades after the repetitive vacuum arc melting. The low oxygen Mo ingot thus can be used as a raw material for sputtering targets.

Effects of Mineral Powder on Performance of Warm Reclaimed Asphalt Mixture

  • Liu, Yao;Wang, Xiao-Yong
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2018.05a
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    • pp.216-217
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    • 2018
  • The three kinds of tests are used to further study the effect of the amount of mineral powder in this mixture design. Firstly, comparing the relationship of the content of mineral powder and asphalt bitumen membrane thickness at different asphalt content, through film thickness to determine the range of gradation and asphalt content in laboratory tests, Grade A and Grade D, asphalt content 2.6%, 3.4% and 3.8% are set for the benchmark, then fatigue properties of the test are carried out in the established range, the result show that asphalt film thickness decreases with the addition of mineral powder. The result also show that fatigue properties of asphalt rubber mixture will reduced, when mineral powder added in, especially when the asphalt content is high.

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Fabrication of Porous Nano Particles from Al-Cu Alloy Nano Powders Prepared by Electrical Wire Explosion (전기선 폭발법으로 제조된 Al-Cu 합금 나노분말을 이용한 다공성 나노 입자 제조)

  • Park, Je-Shin;Kim, Won-Baek;Suh, Chang-Youl;Ahn, Jong-Gwan;Kim, Byoung-Kyu
    • Journal of Powder Materials
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    • v.15 no.3
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    • pp.234-238
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    • 2008
  • Al-Cu alloy nano powders have been produced by the electrical explosion of Cu-plated Al wire. The porous nano particles were prepared by leaching for Al-Cu alloy nano powders in 40wt% NaOH aqueous solution. The surface area of leached powder for 5 hours was 4 times larger than that of original alloy nano powder. It is demonstrated that porous nano particles could be obtained by selective leaching of alloy nano powder. It is expected that porous Cu nano powders can be applied for catalyst of SRM (steam reforming methanol).

Direct Preparation of Fine Nickel Powder by Slurry Reduction Method for MLCC (슬러리환원법에 의한 MLCC용 미세 니켈 분말 직접 제조)

  • Shin, Gi-Wung;Ahn, Jong-Gwan;Kim, Dong-Jin;Kim, Sang-Bae;Ahn, Jea-Woo
    • Journal of the Mineralogical Society of Korea
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    • v.23 no.3
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    • pp.191-197
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    • 2010
  • Fine nickel metal powder of uniform morphology, narrow size distribution, and high purity was prepared from high purity metal solution. Slurry reduction method for the synthesis of metal powder was applied with a special interest in their fine and spherical shape. The products were characterized by scanning electron microscopy (SEM) and X-ray diffraction (XRD). Well dispersed ultrafine nickel powder with the particle size range of 100~200 nm was produced from Ni-hydrazine precursor using hydrazine as a reductant for 90 min reaction in 4.5 M NaOH solution.

The Selective Leaching of Al-Ni Alloy Nano Powders Prepared by Electrical Wire Explosion (전기선 폭발법에 의하여 제조된 Al-Ni 합금 나노분말의 선택적 침출)

  • Park, Je-Shin;Kim, Won-Baek;Suh, Chang-Youl;Chang, Han-Kwon;Ahn, Jong-Gwan;Kim, Byoung-Kyu
    • Journal of Powder Materials
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    • v.15 no.4
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    • pp.308-313
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    • 2008
  • Al-Ni alloy nano powders have been produced by the electrical explosion of Ni-plated Al wire. The porous nano particles were prepared by leaching for Al-Ni alloy nano powders in 20wt% NaOH aqueous solution. The structural properties of leached porous nano powder were investigated by nitrogen physisorption, X-ray diffraction (XRD) and transmission Microscope (TEM). The surface areas of the leached powders were increased with amounts of AI in alloys. The pore size distributions of these powders were exhibited maxima at range of pore diameters 3.0 to 3.5 nm from the desorption isotherm. The maximum values of those were decreased with amounts of Al in alloys.

Ball Milling of Aluminum Foil Scrap (알루미늄 호일 스크랩의 볼밀링)

  • Hong, Seong-Hyeon;Kim, Byeong-Gi
    • 연구논문집
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    • s.29
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    • pp.131-139
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    • 1999
  • The effect of ball milling conditions in the milling of aluminium foil scraps was studied. Initial foil thickness, ball size. content of oleic acid. weight ratio of mineral spirits/foil. charged amount of foil were varied in wet ball milling process. It is impossible to make flake powders by milling of foil scraps with thickness $120 \mum$. As foil thickness decreases from $60\mum$ to $6.5\mum$, Mean size of powder milled for 30 h decreases from 107 µm to 17 µm. Bigger ball is slightly beneficial for milling of foils to the flake powders due to the larger impact energy produced by them. It is impossible to mill the foil without oleic acid to fabricate the flake powder. As content of oleic acid increases from 1.5 % to 5 %, mean size of flake powder milled for 30 h is drastically decreased. For the mineral spirits content below 50 %, foil scrap was not milled because sliding motion of balls by lubricant effect between balls and wall of container. As weight ratio of mineral spirits and foil increase over 100 %, foils were milled powders with mean powder size 15 - 20 때 irrespective of mineral spirits content due to reduced lubricant effect. As charged amount of foil decreases, mean powder size decreases due to increased collision frequency between ball and foil.

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A Study on the Physicochemical Activities of Dangmyon (starch vermicelli) Added with Mulberry Leaves Powder (뽕잎분말을 첨가한 당면의 생리활성 평가)

  • Jeon, Seo Young;Kim, Ae Jeong;Rho, Jeong Ok
    • Korean Journal of Human Ecology
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    • v.24 no.5
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    • pp.713-723
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    • 2015
  • This study was performed to investigate the physicochemical activities such as mineral contents, antioxidantant activities, ${\partial}$-glucosidase activity, and angiotensin I-converting enzyme(ACE) inhibitory effect of Dangmyon (starch vermicelli) prepared with mulberry leaves powder. Mulberry leaves powder was added in ratio (w/w) of 0% (CON), 0.5% (MD1), 1.0% (MD2), 1.5% (MD3), and 2.0% (MD4), and then mineral contents, total polyphenol contents, antioxidant, antidiabetic, and antihypertensive activities of the Dangmyon were measured. The mineral contents were significantly increased by the addition of mulberry leaves powder (p<0.001). The total polyphenol contents and antioxidant activities of Dangmyon were significantly increased by the addition of mulberry leaves powder (p<0.05). In terms of antidiabetic and antihypertensive activities showed MD1~MD4 samples higher contents of ACE and ${\alpha}$-glucosidase compared to control (p<0.05). Our findings suggest that addition of mulberry leaves powder to Dangmyon may improve the effects of anti-oxidation, anti-DM, and anti-hypertension and provide health benefits of consumers.

Synthesis of Flake Ag Powder by Polyol Process (폴리올법에 의한 편상의 은 분말 합성)

  • Kim Dong-Jin;Liang Huanzhen;Ahn Jong-Gwan;Lee Jae-Ryeong;Chung Hun-Saeng
    • Journal of Powder Materials
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    • v.11 no.6 s.47
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    • pp.477-485
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    • 2004
  • Monodispersed flaky silver powder was obtained by controlling the ratios of $H_{2}O_{2}/NH_{3}$ and Agin in a mixed solution of ethylene glycol and ammonia with an addition of PVP. The effects of $NH_{3}/Ag,\; H_{2}O_{2}/Ag\;and\;H_{2}PtCl_{6}/Ag$ on its morphology and size were investigated. In $H_{2}O_{2}-NH_{3}-AgNO_{3}\;system,\;NH_{3}/Ag$ molar ratio was found to be an important reaction factor for the nucleation and crystal growth of Ag powder. The synthesis of flaky powder was optimized at over 6 of $NH_{3}/Ag \;and\;5\;of\;H_{2}O_{2}/Ag\;under\;1.0{\times}10^{-3}\;of\;Pt/Ag.\;Moreover,\;as\;the\; NH_{3}/Ag$ molar ratio increased, the size of precipitates was increased regardless of the amount of Pt. In the absence of $H_{2}PtCI$, the morphology and size of reduced Ag powder were found to be irregular in shape $2-4{\mu}m$ in diameter. However, homogenized fine Ag powder was obtained due to heterogeneous nucleation when $H_{2}PtCI$ used as a cat-alyst, and flaky one was synthesized with the addition of Pt over $1.0{\times}10^{-3}$ of Pt/Ag.