• Title/Summary/Keyword: Silica Preform

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HEAT TRANSFER ANALYSIS ON THE PREFORM HEATING AND THE GLASS FIBER DRAWING IN A GRAPHITE FURNACE FOR OPTICAL FIBER MANUFACTURING PROCESS (광섬유 생산공정용 퍼니스 내의 모재 가열 및 유리섬유 인출에 대한 열전달 해석)

  • Kim, K.;Kim, D.;Kwak, H.S.
    • 한국전산유체공학회:학술대회논문집
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    • 2011.05a
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    • pp.88-91
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    • 2011
  • Glass fiber drawing from a silica preform is one of the most important processes in optical fiber manufacturing. High purify silica preform of cylindrical shape is fed into the graphite furnace, and then a very thin glass fiber of 125 micron diameter is drawn from the softened and heated preform. A computational analysis is performed to investigate the heat transfer characteristics of preform heating and the glass fiber drawing in the furnace. In addition to the dominant radiative heating of preform by the heating element in the furnace, present analysis also includes the convective heat transport by the gas flowing around the preform that experiences neck-dawn profile and the freshly drawn glass fiber at high fiber drawing speed. The computational results present the effects of gas flow on the temperature of preform and glass fiber as well as the neck-down profile of preform.

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Fabrication of $Al_2O_3/Al$ Composites by Replacement Reaction of Molten Metal Al (용융 Al의 치환반응에 의한 $Al_2O_3/Al$ 복합체의 제조)

  • 정두화;김용진;배원태
    • Journal of the Korean Ceramic Society
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    • v.34 no.6
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    • pp.591-600
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    • 1997
  • Al2O3/Al composites were produced by displacement reaction method, which was carried out by immersing the sintered silica preform, which was prepared from fused silica powder, in molten aluminum. Because the molten aluminum did not penetrate into the silica preform with higher than 20% of porosity when the displacement reaction was accomplished at 100$0^{\circ}C$ for 10 hours in air atmosphere, the optimum range of sintering temperature of silica preform was from 135$0^{\circ}C$ to 140$0^{\circ}C$. The microstructure of this Al2O3/Al composites showed three-dimentionally co-continuous alumina, which provides wear resistance and high stiffness, and aluminium which acts as a toughnening phase. The grain size of the alumina in composites did not change with the particle size of the silica preform. The exact shape of the preform was retained and a net-shaped composite was produced. The representative Al2O3/Al composite prepared in this study showed 3.30mg/㎤ of bulk density, 350-430 MPa of flexural strength, 7.0 MPa.m1/2 of fracture toughness, and good machinability.

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RADIATIVE HEAT TRANSFER ANALYSIS OF GLASS FIBER DRAWING IN OPTICAL FIBER MANUFACTURING (광섬유 생산용 유리섬유 인출공정에 대한 복사 열전달 해석)

  • Kim, K.;Kim, D.;Kwak, H.S.
    • Journal of computational fluids engineering
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    • v.16 no.1
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    • pp.22-29
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    • 2011
  • In this study, the glass fiber drawing from a silica preform in the furnace for the optical fiber manufacturing process is numerically simulated by considering the radiative heating of cylindrically shaped preform. The one-dimensional governing equations of the mass, momentum, and energy conservation for the heated and softened preform are solved as a set of the boundary value problems along with the radiative transfer approximation between the muffle tube and the deformed preform shape, while the furnace heating is modeled by prescribing the temperature distribution of muffle tube. The temperature-dependent viscosity of silica plays an important role in formation of preform neck-down profile when the glass fiber is drawn at high speed. The calculated neck-down profile of preform and the draw tension are found to be reasonable and comparable to the actual results observed in the optical fiber industry. This paper also presents the effects of key operating parameters such as the muffle tube temperature distribution and the fiber drawing speed on the preform neck-down profile and the draw tension. Draw tension varies drastically even with the small change of furnace heating conditions such as maximum heating temperature and heating width, and the fine adjustment of furnace heating is required in order to maintain the appropriate draw tension of 100~200 g.

Effects of Metal Mg on Replacement Reaction of Molten Al for Fabrication of $Al_2$O$_3$//Al Composites (Al$_2$O$_3$/Al 복합체 제조시 용융 알루미늄의 치환반응에 미치는 금속 마그네슘의 영향)

  • 정두화;배원태
    • Journal of the Korean Ceramic Society
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    • v.35 no.1
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    • pp.23-32
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    • 1998
  • Al2O3/Al composites were produced by immersing the sintered silica preform in molten aluminum which contained magnesium as impurity. Three distinct regions existed in the penetration behavior of molten me-tal with changing the reaction temperature. These regions are denoted as low temperature regime(75$0^{\circ}C$-85$0^{\circ}C$) intermediate regime(90$0^{\circ}C$-95$0^{\circ}C$) and high temperature regime(100$0^{\circ}C$$\leq$) In the low temperature regime the penetration speed of molten aluminum increased with increasing reaction temperature whereas it decreased in the intermediate regime due to the phase transition of alumina formed by displacement reac-tion. In the high temperature regime the penetration speed of molten aluminum was the highest at 100$0^{\circ}C$ which was 3.6 mm/hr But above 105$0^{\circ}C$ molten aluminum did not penetrate into the silica preform because of the formation of a dense spinel layer at the preform surface by magnesium in molten Al.

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Study on the Fabrication Process of Polarization Maintaining Photonic Crystal Fibers and Their Optical Properties

  • Cho, Tai-Yong;Kim, Gil-Hwan;Lee, Kwan-Il;Lee, Sang-Bae;Jeong, Je-Myung
    • Journal of the Optical Society of Korea
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    • v.12 no.1
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    • pp.19-24
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    • 2008
  • In this paper, we describe the fabrication process and the characteristics of polarization maintaining photonic crystal fibers (PM-PCFs). The PM-PCF is fabricated by stack-and-draw method, i.e., stacking silica capillary tubes (making a PM-PCF preform) and drawing to optical fiber. Firstly, a PM-PCF preform is formed by stacking two kinds of capillary tubes around a solid silica rod and jacketing these stacked tubes with an outer silica tube (out-jacket tube). Later, the desired preform is drawn to a fiber in a high temperature drawing tower. We also compare the polarization properties such as polarization dependent loss, birefringence, and differential group delay of the fabricated PM-PCF with those of the conventional PANDA PM fiber.

COMPUTATIONAL STUDY OF GLASS FIBER DRAWING PROCESS IN A DRAW FURNACE OF OPTICAL FIBER MASS MANUFACTURING SYSTEM (광섬유 대량생산용 인출퍼니스 내 유리섬유 인출공정의 전산해석)

  • Kim, K.;Kwak, H.S.;Kim, D.
    • Journal of computational fluids engineering
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    • v.18 no.4
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    • pp.69-73
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    • 2013
  • Mass manufacturing of optical fiber includes the process of very thin glass fiber drawing by heating and softening the high purity silica preform and applying the draw tension on the softened tip of preform neck-down profile in a draw furnace. In this computational study, this process is numerically modeled with simplified geometry of the draw furnace which is comprised of essential parts such as concentric graphite heater, muffle tube, and insulation surrounding the heater. The iterative computational scheme is employed between one-dimensional model of neck-down profile prediction and two-dimensional axisymmetric thermo-fluid CFD computation of radiative heating and working gas convection. The computational results show the experimentally observed neck-down profile in heated section of preform, while yielding the reasonable values of draw tension and heater wattage. Also, this study analyzes and discusses the effects of heating conditions such as heater length and temperature on several important aspects of glass fiber drawing process.

Al2O3/Al Composites Fabricated by Reaction between Sintered SiO2 and Molten Al (실리카 소결체와 용융 알루미늄과의 반응에 의한 $Al_2$O$_3$/Al 복합체의 제조)

  • 정두화;배원태
    • Journal of the Korean Ceramic Society
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    • v.35 no.9
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    • pp.923-932
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    • 1998
  • Al2O3/Al composites were produced by displacement reaction method which was carried out by imm-ersing the sintered silica preform which was prepared form fused silica powder in molten aluminu. an ac-tivation energy of 94kJ/mole was calculated from Al-SiO2 reaction data in 1000-130$0^{\circ}C$ temperature range With increase of reaction temperature the alumina particle in the Al2O3/Al composites produced with pur metal Al showed grain growth and the growth of alumina particle in Al2O3/Al composite produced by using of Mg contained Al alloy was inhibited. The flexural strength of Al2O3/Al composites produced at 100$0^{\circ}C$ showed the highest value as 393 MPa. Flexural strength of the composite fabricated at 85$0^{\circ}C$ showed higher deviation than that of the composite produced at above 100$0^{\circ}C$ Low flexural strength of the composite fa-bricated at 120$0^{\circ}C$ due to the growth of pore and alumina particle size. The hardness of composites de-pended on alumina content in Al2O3/Al composite decreased with increasing of aluminium content in case the same alumina content and increased with increasing of silicon content in composite.

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Fabrication and mechanical properties of $Al/Al_2O_3$ composites by reactive metal penetration method (반응 금속 침투법에 의한 $Al/Al_2O_3$복합체의 제조 및 기계적 특성)

  • 윤영훈;홍상우;최성철
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.11 no.6
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    • pp.239-245
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    • 2001
  • $Al/Al_2O_3$composites were prepared from the reaction of mullite preforms and amorphous silica in aluminum melt at $1100^{\circ}C$ for 5 hrs. The chemical reaction between mullite preform and aluminum melt has formed the interconnected microstructure. The metal content of $Al/Al_2O_3$composite was controlled with the variable of the apparent porosity according to the sintering temperature of mullite preforms; $1600^{\circ}C$,$ 1625^{\circ}C$, $1650^{\circ}C$ and $1700^{\circ}C$, the mechanical properties of $Al/Al_2O_3$composite were investigated upon the content of Al. The mullite preform sintered above $1600^{\circ}C$ showed the chemical reaction with the penetrated Al melt, but the mullite sintered at $1600^{\circ}C$ didnt react with aluminum melt owing to the non-wetting of Al melt/mullite preform. The influences of penetration direction on the mechanical properties of composites were considered with the two different models of the perpendicular pattern and the parallel pattern to the direction of Al melt penetration. With the increase of Al metal penetration content, the fracture strength of $Al/Al_2O_3$composite decreased and the fracture toughness of composite increased. The microstructure of $Al/Al_2O_3$composite was determined by the direction of metal penetration, but the fracture strength and fracture toughness of composite didnt show the dependence on metal penetration direction.

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Fiber Drawing Induced Defects in Silica Optical Fiber (광섬유 인선 공정에 의해 생성된 실리카 광섬유내 점결함)

  • 안병길;이종원;김효태
    • Journal of the Korean Ceramic Society
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    • v.40 no.11
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    • pp.1102-1105
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    • 2003
  • The fiber drawing process induced defects in silica fiber have been investigated. This study has focused on the Oxygen Deficient Centers (ODCs) and E' centers induced by the fiberization process in low-OH silica fibers. To investigate those defects induced by the fiberization process, the optical absorption spectrum and Electron Spin Resonance (ESR) have both been employed. The concentration of Oxygen Deficient Centers (ODCs) and E' centers are increased by the fiber drawing process. The population of defects in the neck-down region has also been investigated. The most significant generation of defects during fiber drawing process has been shown to occur in this region of silica preform. The population of defects is higher on the edge region than in the center of neck-down region.

Analysis of residual thermal stress in an aluminosilicate core and silica cladding optical fiber preform

  • Shin, Woo-Jin;K. Oh
    • Proceedings of the Optical Society of Korea Conference
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    • 2000.02a
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    • pp.214-215
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    • 2000
  • As silica based optical fibers and preforms are processed at a high temperature, residual stresses are bulit in the strucure when cooled down to the room temperature. The magnitude of the residual stress depends on the difference in the thermal expansion coefficients between core and cladding glass as well as on the temperature difference. Residual stress distribution determines the intrinsic strength and could affect the long term reliability of optical fibers. And furthermore, stress can introduces anisotropy into optical fibers by photoelastic effects. The analysis of thermal stress has been intensively studied for multimode fibers$^{(1)}$ and the authors and co-wokers recently reported the stress distribution in a depressed inner cladding structure$^{(2)}$ . The compositions of the glass in the previous studies, however, have been restricted to conventional glass formers, such as GeO2, B2O3, P2O5, Fluorine. (omitted)

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