• International Journal of Korean Welding Society
• /
• v.2 no.1
• /
• pp.25-28
• /
• 2002

In the coarse grain HAZ adjacent to the fusion line, most of the TiN particles in conventional Ti added steel are dissolved and austenite grain growth is easily occurred during welding process. To avoid this difficulty, thermal stability of TiN particle is improved by increasing the nitrogen content in steel. In this study, the effect of hlgh nitrogen TiN particle on preventing austenite grain growth in HAZ was investigated. Increased thermal stability of TiN particle is helpful for preventing the austenite grain growth by pinning effect. High nitrogen TiN particle in simulated HAZ were not dissolved even at high temperature such as 1400'E and prevented the austenite grain growth in simulated HAZ. Owing to small austenite grain size in HAZ the width of coarse grain HAZ in high nitrogen TiN steel was decreased to 1/10 of conventional TiN steel. Even high heat input welding, the microstructure of coarse grain HAZ consisted of fine polygonal ferrite and pearlite and toughness of coarse grain HAZ was significantly improved.

• Proceedings of the KWS Conference
• /
• 2002.10a
• /
• pp.217-221
• /
• 2002

In the coarse grain HAZ adjacent to the fusion line, most of the TiN particles in conventional Ti added steel are dissolved and austenite grain growth is easily occupied during welding process. To avoid this difficulty, thermal stability of TiN particle is improved by increasing the nitrogen content in steel. In this study, the effect of high nitrogen TiN particle on preventing austenite grain growth in HAZ was investigated. Increased thermal stability of TiN particle is helpful for preventing the austenite grain growth by pinning effect. High nitrogen TiN particle in simulated HAZ were not dissolved even at high temperature such as 1400 C and prevented the austenite grain growth in simulated HAZ. Owing to small austenite grain size in HAZ the width of coarse grain HAZ in high nitrogen TiN steel was decreased to 1/10 of conventional TiN steel. Even high heat input welding, the microstructure of coarse grain HAZ consisted of fine polygonal ferrite and pearlite and toughness of coarse grain HAZ was significantly improved.

• Journal of Welding and Joining
• /
• v.35 no.1
• /
• pp.9-15
• /
• 2017

IMicrostructure evolution and tensile property in the weld heat-affected zone (HAZ) of austenitic Fe-30Mn-9Al-0.9C lightweight steels were investigated. Five alloys with different V and Nb content were prepared by vacuum induction melting and hot rolling process. The HAZ samples were simulated by a Gleeble simulator with welding condition of 300kJ/cm heat input and HAZ peak temperatures of $1150^{\circ}C$ and $1250^{\circ}C$. Microstructures of base steels and HAZ samples were observed by scanning electron microscopy (SEM) and transmission electron microscopy (TEM), and their mechanical properties were evaluated by tensile tests. The addition of V and Nb formed fine V and/or Nb-rich carbides, and these carbides increased tensile and yield strength of base steels by grain refinement and precipitation hardening. During thermal cycle for HAZ simulation, the grain growth occurred and the ordered carbide (${\kappa}-carbide$) formed in the HAZs. The yield strength of HAZ samples (HAZ 1) simulated in $1150^{\circ}C$ peak temperature was higher as compared to the base steel due to the formation of ${\kappa}-carbide$, while the yield strength of the HAZ samples (HAZ 2) simulated in $1250^{\circ}C$ decreased as compared to HAZ 1 due to the excessive grain growth.

• Journal of Welding and Joining
• /
• v.4 no.2
• /
• pp.40-46
• /
• 1986

This investigation is concerned with the toughness and microstructure of manneristically simulated HAZ in 12% Cr steel. Unnotched specimens were subjected to weld thermal cycles a weld simulator. The parameters-peak temperatures, cooling rate, influence of PWHT and plastic deformation were considered. After weld simulation, the specimens were heat-treated, V-notched and impact tested. An optical metallographic examination was performed to correlate the HAZ toughness with microstructure. Also a fractographic examination was done to obtain information on the fracture mode. The toughness of the coarse grained zone and the part of HAZ subjected to a peak temperature range 700-800.deg. C are lower than the other parts. However, they are still high enough. The double PWHT cycle could not improve the HAZ toughness in present study. However, if the first PWHT is conducted before the work piece is cooled below $M_f$, it is expected that the double PWHA may be beneficial to the toughness of the HAZ. It is also expected that martensitic welding can be used on production welds.

• International Journal of Korean Welding Society
• /
• v.3 no.2
• /
• pp.40-45
• /
• 2003

A series of experiments has been carried out to investigate the effect of titanium, boron and nitrogen on the microstructure and toughness of simulated heat affected zone (HAZ) in quenched and tempered (QT) type 490MPa yield strength steels. For acquiring the same strength level, the carbon content and carbon equivalent could be lowered remarkably with a small titanium and boron addition due to the hardenability effect of boron during quenching process. Following the thermal cycle of large heat input, the coarsened grain HAZ (CGHAZ) of conventional quenched and tempered (QT) type 490MPa yield strength steels exhibited a coarse bainitic or ferrite side plate structure with large prior austenite grains. While, titanium and boron bearing QT type 490MPa yield strength steels were characterized by the microstructure in the CGHAZ, consisting mainly of the fine intragranular ferrite microstructure. Toughness of the simulated HAZ was mainly controlled by the proper Ceq level, and the ratio of Ti/N rather than titanium and nitrogen contents themselves. In the titanium­boron added QT steels, the optimum Ti/N ratio for excellent HAZ toughness was around 2.0, which was much lower than the known Ti/N stoichiometric ratio, 3.4. With reducing Ti/N ratio from the stoichiometric ratio, austenite grain size in the coarse grained HAZ became finer, indicating that the effective fine precipitates could be sufficiently obtained even with lower Ti/N level by adding boron simultaneously. Along with typical titanium carbo­nitrides, various forms of complex titanium­ and boron­based precipitates, like TiN­MnS­BN, were often observed in the simulated CGHAZ, which may act as stable nuclei for ferrite during cooling of weld thermal cycles

• Proceedings of the KWS Conference
• /
• 2002.10a
• /
• pp.38-42
• /
• 2002

HAZ(Heat Affected Zone of weldm ents) properties were investigated for a high nitrogen austenitic stainless steel with a chemical composition of Fe-0.02C-0.15Si-6.00Mn-10.0Ni-23.0Cr-2.00Mo-0.48N-0.14V. Thermal cycle of HAZ was simulated by the thermal cycle simulator (Gleeble 1500). The heat treatment was applied to the Charpy test size sample without notch under various peak temperatures and/or the holding times condition. V-notch Charpy test was performed at the temperature range of 273~77 K. Metallographic examination also was carried out by using optical microscopy, scanning electron microscopy and transmission electron microscopy. The simulated specimens revealed a slight embrittlement compared with the base materials. The impact toughness of the specimens deteriorated with the decreasing test temperature. The results from Charpy V-notch test, however, showed that significant degradation of absorbed energy caused by brittle fracture was not observed for the specimen tested in the test temperature range.

• Journal of Welding and Joining
• /
• v.20 no.3
• /
• pp.91-97
• /
• 2002

Variation of HAZ toughness of Ti-containing steel with nitrogen content was investigated and interpreted in terms of its microstructure and the amount of soluble nitrogen present. The amounts of Ti and Al combined in TiN and AlN, respectively, in HAZ at $1400^{\circ}C$ peak temperature were less than those in base plate; 55~88% in TiN and 21~28% in AlN, indicating the dissolution of nitrifies in HAZ. The calculated amounts of soluble nitrogen using the thermodynamic analysis showed a good agreement with the measured values in other experiment. Therefore, the analysis can be used to estimate the amount of soluble nitrogen in HAZ. Simulated HAZ toughness was influenced not only by its microstructure but also by the amount of soluble nitrogen present after the formation of BN during the cooling cycle of welding. It showed maximum value when the nitrogen content is in stoichiometric ratio with titanium content, showing that soluble nitrogen in HAZ is detrimental to its toughness.

• Journal of Welding and Joining
• /
• v.5 no.1
• /
• pp.73-80
• /
• 1987

During PWHT, it is well known that residual stress in weld HAZ is one of the reasons for PWHT embitterment. In case of static loading, it was experimentally found that fracture toughness of weld HAZ was dependant upon PWHT conditions. However, the effects of PWHT on fatigue behavior are not clearly verified. Therefore, in this paper, the effects of heating rate PWHT conditions and residual stress simulated in weld HAZ of Cr-Mo steel on fatigue crack propagation behavior were evaluated by fatigue Testing and SEM observation. The obtained results are summarized as follows; 1. Applied stress($10 Kgf/mm^2$) in weld HAZ during PWHT tneded to decrease fatigue strength and to increase fatigue crack growth rate. 2. Applied stress and slow heating rate of 60.deg. C/hr during PWHT contributed to precipitin of impurity elements as well as carbide, which promoted the fatigue crack growth. 3. Fatigue crack growth rate decreased at the heating rate of 220.deg. C/hr in contrast with 600.deg. C/hr and 60.deg. C/hr.

• Proceedings of the KSME Conference
• /
• 2000.11a
• /
• pp.322-327
• /
• 2000

This paper investigates the time-dependent crack growth in X20CrMoV 12 1 steel weld joints. Crack growth test are carried out $545^{\circ}C$ on side-grooved 1/2T CT specimens under static loads. A simulated material is produced for the intercritical HAZ, where fracture normally occurs. Constitutive properties are obtained for the simulated HAZ material as well as for the base metal and weld metal. Finite element analyses of crack growth are performed on the models with and without a HAZ layer, using the experimental crack length-time history. The inclusion of HAZ layer increase the load line velocities significantly. The crack growth rates are correlated reasonably well with $C^*$. The smallest crack size for the validity of $C^*$ is found much smaller than the ASTM crack initiation size for 1T CT specimen of creep ductile materials.

• Proceedings of the KWS Conference
• /
• 2002.10a
• /
• pp.714-719
• /
• 2002

In The Great Hanshin-Awaji Earthquake, the general yield brittle fractures were observed in beam-column connections of steel building frames. Among many influencing factors which affect the general yield brittle fracture, it can be considered that fracture toughness has substantial effects. Some studies are making clear the required toughness for the base metal and the weld metal, but general values are not proposed. Moreover, it seems that it is also important to pay attention to the toughness decrease in the weld heat affected zone (weld HAZ), because the toughness decrease occurs in the HAZs of mild steel. In this paper, the relationship between toughness of simulated HAZs of "the rolled steels for building structures (SN)" and the weld heat-input limit of the SN steel are investigated, in an attempt to provide the required toughness for HAZs. The relationships between the increase of the hardness value and toughness, and changes of microstructure after weld heat-input are also discussed. The main results are summarized as follows. 1) The SN400B can keep its toughness at higher heat-inputs compare to the SN490Bs. 2) The steel grade, which becomes harder than other steel grades at the same heat-input, has smaller absorbed energy and smaller limit of heat-input. 3) The weld heat-input limit of the SN400B and the SN490B are proposed separately for some required toughness values.