• Title/Summary/Keyword: electrospray

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Characteristics of the electrospraying combustion using grooved nozzle (홈노즐을 이용한 정전분무 확산 연소 특성에 관한 연구)

  • Kim, Woo-Jin;Kim, Kyoung-Tae;Kim, Sang-Soo
    • Proceedings of the KSME Conference
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    • 2007.05b
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    • pp.2366-2371
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    • 2007
  • Spray combustion characteristics of a conducting fuel electrospray have been studied for clean combustion technology. The multiplexing system which can retain the characteristics of the cone-jet mode is inevitable for the electrospray application. Charged micro droplets can be obtained in almost uniform size during operating the electrospray in the cone-jet mode. This experiment device set up the multiplexed grooved nozzle system with the extractor. Using the grooved nozzle, the stable cone-jet mode can be achieved at the each groove in the grooved mode. This electrospray system was applied to the diffusion combustion. It is the first step to discover the diffusion combustion characteristics of the electrospray. In case of the single grooved nozzle electrospray, the diffusion flames are occurred at each jet of grooved mode and they are quite stable. The exhaust gas analysis was indicated that there is the critical point which can make very stable diffusion combustion.

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Characteristics of the Electrospraying Combustion Using Grooved Nozzle (홈노즐을 이용한 정전분무 확산 연소 시스템 개발 및 특성 연구)

  • Kim, Woo-Jin;Kim, Kyoung-Tae;Kim, Sang-Soo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.31 no.12
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    • pp.979-985
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    • 2007
  • Spray combustion characteristics of the conducting fuel electrospray has been studied for clean combustion technology. The electrospraying multiplexed system which can maintain the characteristics of the cone-jet mode is able to obtain charged micro droplets with high flow rate. In addition, they have monodisperse distribution during operating the electrospray in the cone-jet mode. The multiplexed grooved nozzle system with the extractor was applied to this experimental device set up. The stable grooved mode can be generated by the grooved nozzle and this electrospray system was applied to the diffusion combustion. It is the first step to discover the diffusion combustion characteristics of the electrospray, In case of the single grooved nozzle electrospray the diffusion flames are occurred at each Jet of grooved mode and they are quite stable. The exhaust gas analysis was indicated that there is the critical point which can make very stable diffusion combustion

Dual Nano-Electrospray and Mixing in the Taylor Cone

  • Radionova, Anna;Greenwood, David R.;Willmott, Geoff R.;Derrick, Peter J.
    • Mass Spectrometry Letters
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    • v.7 no.1
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    • pp.21-25
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    • 2016
  • Dual-channel nano-electrospray has recently become an ionization technique of great promise especially in biological mass spectrometry. This unique approach takes advantage of the mixing processes that occurs during electrospray. Understanding in more detail the fundamental principles influencing spray formation further study of the origins of the mixing processes: (1) in a Taylor cone region, (2) in charged droplets or (3) in both environments. The dual-channel emitters were made from borosilicate theta-shape glass tubes (O.D. 1.2 mm) and had a tip diameters of less than 4 μm. Electrical contact was achived by deposition of a thin film of an appropriate metal onto the surface of the emitter. The experimental investigation of the Taylor cone formation in a dual-channel electrospray emitter has been carried out by injection of polystyrene beads (diameter 3 μm) at very low concentrations into one of the channels of the non-tapered theta-glass tubes. High-speed camera experiments were set up to visualize the mixing processes in Taylor cone regions for dual-channel emitters. Mass spectra from dual nano-electrospray are presented.

Characteristics of Multiplexed Grooved Nozzles for High Flow Rate Electrospray (고유량 정전분무를 위한 다중 홈노즐 특성 연구)

  • Kim, Kyoung-Tae;Kim, Woo-Jin;Kim, Sang-Soo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.31 no.10
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    • pp.848-854
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    • 2007
  • The electrospray operated in the cone-jet mode can generate highly charged micro droplets in an almost uniform size at low flow rates. Therefore, the multiplexing system which can retain the characteristics of the cone-jet mode is inevitable for the electrospray application. This experiment reports the multiplexed grooved nozzle system with the extractor. The effects of the grooves and the extractor on the performance of the electrospray were evaluated through experiments. Using the grooved nozzle, the stable cone-jet mode can be achieved at the each groove in the grooved mode. Furthermore, the number of nozzles per unit area is increased by the extractor. The multiplexing density is 12 jets per $cm^2$ at 30 mm distance from the nozzle tip to the ground plate. The multiplexing system for the high flow rate electrospray is realized with the extractor which can diminish the space charge effect without sacrificing characteristics of the cone-jet mode.

Experimental Study on the Enhancement of Particle Removal Efficiency in Spray Tower Scrubber Using Electrospray

  • Kim, Hyeok-Gyu;Kim, Hong-Jik;Lee, Myong-Hwa;Kim, Jong-Ho
    • Asian Journal of Atmospheric Environment
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    • v.8 no.2
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    • pp.89-95
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    • 2014
  • There have been a lot of efforts to keep permissible emission standards and to reduce the amount of emitted air pollutants. There are several air pollution control equipments, however, wet scrubber is used to remove particulate matters and gaseous pollutants simultaneously, even if it has low collection efficiency in the particle size less than $5.0{\mu}m$. To overcome this problem, we introduced a spray tower scrubber with an electrospray system which a high voltage was indirectly applied. We found that collection efficiency of fine particles in the electrospray system was improved by increasing electrical field strength and the ratio of liquid-gas flow rate (from 41% to 84% for $0.3{\mu}m$ particles). In addition, a number of small droplets generated from an electrospray system led high collection efficiency, resulting from electrostatic attraction between droplets and particles and higher collision frequency. Therefore, we can conclude that the introduction of an electrospray system is quite effective to increase the particle removal efficiency of a spray tower scrubber.

Sheathless electrospray ionization with integrated metal emitter on microfluidic device (전기 분무 이온화를 이용한 단백질 질량분석용 마이크로 유체 소자의 제작 및 실험)

  • Kim, Min-Su;Joo, Hwang-Soo;Lee, Kook-Nyung;Kim, Byung-Gee;Kim, Yong-Kweon
    • Proceedings of the KIEE Conference
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    • 2004.07c
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    • pp.2102-2104
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    • 2004
  • In this study, sheathless electrospray from PDMS/glass microchips with conducting metal emitter tip is described. A chip-based capillary electrophoresis/mass spectrometry (CE/MS) system has advantages of the CE separation and on-line electrospray detection of peptide solution. We have fabricated a new electrospray ionization(ESI) device composed of the metal emitter tip and CE separation channel monolithically in a glass microchip. The separation channel and metal emitter tip are fabricated using a glass wet etching and gold electro plating process, respectively. The fabricated micro electrospray chip was tested by spraying peptide sample for mass spectrometric analysis. Singlely-charged peak and doublely-charged peak of peptide were detected and further MS/MS fragmentation was performed in each peak. Direct comparisons with conventional glass or fused silica emitters showed very similar performance with respect to signal strength and stability.

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Collection Efficiency Enhancement of Spray Tower Scrubber by Introducing Electrospray with Two-flow Nozzle (분무탑식 스크러버에서 이류체 정전분무에 의한 집진효율의 향상)

  • Hwang, You-Seong;Kim, Jong-Ho;Kim, Jong-Hyeon
    • Journal of Korean Society for Atmospheric Environment
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    • v.26 no.3
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    • pp.339-345
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    • 2010
  • There have been a number of efforts to satisfy national emission regulations and reduce the amount of emitted air pollutants. There are several air pollution control devices, however, only wet scrubber is efficiently used to remove particulate matters and gaseous pollutants, even if it has minimum collection efficiency in the particle size range of $0.1{\sim}1{\mu}m$. This study aimed to improve the collection efficiency of a spray tower type scrubber by introducing an electrospray system with two-flow nozzle. We found that the collection efficiency of a spray tower type scrubber was similar to that of a conventional wet scrubber. However, installation of an electrospray system in the scrubber resulted in drastic further improvement of collection efficiency comparing to that of a conventional scrubber, which is 26%, 35.2%, and 45.1% at the liquid to gas ratio of 0.26 $L/m^3$ and 19.9%, 35.1%, and 42.5% at 0.34 $L/m^3$ for the applied voltage of -30 kV, -35 kV, and -40 kV, respectively. Therefore, we found that the introduction of an electrospray system is very effective to improve the collection efficiency of a spray tower type scrubber.

Variation of Nutrient Broth Droplets Patterned by Electrospray System with Flow Rates (정전분무를 이용한 패턴화된 생물현탁액 액적의 유량에 따른 변화 연구)

  • Jeong, Sang Bin;Jang, Kyung Soo;Lee, Gunwoong;Chong, Euiseok;Heo, Ki Joon;Lee, Byung Uk
    • Particle and aerosol research
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    • v.11 no.4
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    • pp.115-118
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    • 2015
  • An electrospray patterning method has been considered as a new and effective way for controlling very fine droplets. Drop-on-demand patterning for unstained nutrient broth on wafers was newly conducted with an electrospray pulsed jet. The patterns had been made under varying experimental conditions including flow rate, vibration frequency, and translational speed of the electrospray patterning system. In this experiment, especially, variation of nutrient broth droplet was measured under varying flow rate conditions. This new technique has a potential to be applied in biology experiments and hormone medical industry.

Preparation of C-plane oriented BaFe12O19 film by electrospray deposition of colloidal precursor particles (정전분무 장치를 이용한 C축 일방향 바륨페라이트(BaFe12O19) 박막형성)

  • Lee, Hye Moon;Kim, Yong Jin
    • Particle and aerosol research
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    • v.6 no.1
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    • pp.21-27
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    • 2010
  • New process consisting of electrospray and epitaxial crystal growth processes was applied to the preparation of c-plane oriented barium ferrite ($BaFe_{12}O_{19}$) thin film for high density magnetic recording media. Sodium citrate aided process was proper to preparation of amorphous $BaFe_{12}O_{19}$ nanoparticles with geometric mean diameter of 3 nm and geometric standard deviation of 1.1. The electrospray was applicable to the prepare of amorphous $BaFe_{12}O_{19}$ thin film on a substrate, and the film thickness could be controlled by adjusting the electrospray deposition time. The c-plane oriented $BaFe_{12}O_{19}$ thin film was successfully prepared by 3 step annealing process of the $BaFe_{12}O_{19}$ amorphous film on a sapphire($Al_2O_3$) substrate; annealing at $350^{\circ}C$ for 30 min, annealing at $500^{\circ}C$ for 30 min, and annealing at $700^{\circ}C$ for 60 min.

Mass spectrometry analysis system with integrated micro electrospray ionization emitter for peptide detection (펩타이드 질량 분석을 위한 전기 이온화 분사기의 제작 및 성능 평가)

  • Kim, Min-Su;Joo, Hwang-Soo;Kim, Byung-Gee;Kim, Yong-Kweon
    • Proceedings of the KIEE Conference
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    • 2007.07a
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    • pp.1534-1535
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    • 2007
  • This paper describes a novel microfluidic device with a microfabricated electrospray source for a sheathless electrospray ionization interface to a mass spectrometer. This electrospray ionization-mass spectrometry (ESI-MS) device consists of a triangular-shaped metal emitter, allowing the generation of an efficient electrospray for peptide detection, and microfluidic channels monolithically in a glass microchip. The performance of the proposed interface was evaluated by opimizing its experimental condition and spraying standard peptides. The spraying has high signal strength and stability, with a relative standard deviation of 2.9% and singly-charged and doubly-charged peaks of the peptides were successfully detected. The metal emitter source showed a good performance to be comparable to commercially available emitters in signal strength and stability.

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